Počet záznamů: 1  

Characterization and crystal structures of new Schiff base macrocyclic compounds

  1. 1. 0456817 - FZU-D 2016 RIV RU eng J - Článek v odborném periodiku
    Khalaji, A.D. - Ghoran, S.H. - Pojarová, Michaela - Dušek, Michal
    Characterization and crystal structures of new Schiff base macrocyclic compounds.
    Journal of Structural Chemistry. Roč. 56, č. 7 (2015), s. 1410-1414. ISSN 0022-4766
    Grant CEP: GA ČR(CZ) GA14-03276S
    Institucionální podpora: RVO:68378271
    Klíčová slova: synthesis * macrocyclic Schiff base * single crystal structure analysis * spectroscopy
    Kód oboru RIV: BM - Fyzika pevných látek a magnetismus
    Impakt faktor: 0.536, rok: 2015

    We report the synthesis and characterization of two new macrocyclic Schiff base compounds: a 15-membered (1) and 16-membered (2) one. Their synthesis involves a Schiff base condensation of 2,2-dimethylpropanediamine and two dialdehydes: 5,5′-dimethoxy-2,2′-(ethane-1,2-diyldioxy)dibenzaldehyde and 5,5′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzaldehyde. The compounds are characterized by elemental analysis (CHN), FT-IR, 1H and 13C-NMR spectroscopy, and single crystal X-ray diffraction.
    Trvalý link: http://hdl.handle.net/11104/0257289