0435389 - ÚFM 2015 RIV NL eng J - Článek v odborném periodiku
Jirásková, Yvonna - Buršík, Jiří - Zitovski, O. - Cuda, J.
Influence of Fe2O3 on alloying and magnetic properties of Fe–Al.
Materials Science and Engineering B-Advanced Functional Solid-State Materials. Roč. 186, AUG (2014), s. 73-78. ISSN 0921-5107. E-ISSN 1873-4944
Grant CEP: GA ČR(CZ) GAP108/11/1350; GA MŠMT 7AMB12SK009
Institucionální podpora: RVO:68081723
Klíčová slova: Fe–Al alloy * Mechanical alloying * Microstructure * Intergrain interaction * magnetic properties
Kód oboru RIV: BM - Fyzika pevných látek a magnetismus; BM - Fyzika pevných látek a magnetismus (UFM-A)
Impakt faktor: 2.169, rok: 2014 ; AIS: 0.475, rok: 2014
DOI: https://doi.org/10.1016/j.mseb.2014.03.012

The present study is devoted to changes of the magnetic properties during the high-energy ball milling of the Fe, Al and Fe2O3 powders. The magnetic properties are supported by the structure morphology, phase composition, and changes in atomic ordering investigated using the structure sensitive scanning electron microscopy, X-ray diffraction and Mössbauer spectrometry. Intergrain exchange coupling results in negative values of ıM(H) Henkel graphs yielding dipolar interactions among particles and only slightly depending on the milling time. The bcc-Fe–Al is detected after 2 h of milling coexisting with the -(Fe,Al)2O3, superparamagnetic oxides, and -Fe. In the next milling steps the changes in the phase composition are seen. While a small amount of the superparamagnetic oxides and the bcc-Fe–Al phase are detected after 20 h, the -(Fe,Al)2O3 has been dissolved. An increase in the hyperfine induction and saturation magnetization evidences a decrease in Al content in the bcc-Fe–Al estimated to be bellow 18 at.% Al.
Trvalý link: http://hdl.handle.net/11104/0239318