Počet záznamů: 1
Titania-coated manganite nanoparticles: synthesis of the shell, characterization and MRI properties
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SYSNO ASEP 0473952 Druh ASEP J - Článek v odborném periodiku Zařazení RIV J - Článek v odborném periodiku Poddruh J Článek ve WOS Název Titania-coated manganite nanoparticles: synthesis of the shell, characterization and MRI properties Tvůrce(i) Jirák, Zdeněk (FZU-D) RID, ORCID, SAI
Kuličková, Jarmila (FZU-D) ORCID
Herynek, Vít (UEM-P)
Maryško, Miroslav (FZU-D) RID
Koktan, Jakub (FZU-D) RID
Kaman, Ondřej (FZU-D) RID, ORCIDCelkový počet autorů 6 Zdroj.dok. Journal of Magnetism and Magnetic Materials. - : Elsevier - ISSN 0304-8853
Roč. 427, Apr (2017), s. 245-250Poč.str. 6 s. Jazyk dok. eng - angličtina Země vyd. NL - Nizozemsko Klíč. slova magnetic nanoparticles ; core-shell nanoparticles ; titania coating ; perovskite manganite ; magnetic resonance imaging ; transverse relaxivity Vědní obor RIV BM - Fyzika pevných látek a magnetismus Obor OECD Condensed matter physics (including formerly solid state physics, supercond.) CEP GA15-10088S GA ČR - Grantová agentura ČR GA16-04340S GA ČR - Grantová agentura ČR Institucionální podpora FZU-D - RVO:68378271 ; UEM-P - RVO:68378041 UT WOS 000397199400044 EID SCOPUS 85005993324 DOI 10.1016/j.jmmm.2016.10.097 Anotace Novel procedure for coating of oxide nanoparticles with titania is developed and applied to magnetic cores of perovskite manganite. Bare particles of the ferromagnetic La0.65Sr0.35MnO3 phase, possessing high magnetization, M10 kOe(4.5 K) = 63.5 emu g-1, and Curie temperature, TC = 355 K, are synthesized by sol-gel procedure and subsequently coated with titania. Further, a comparative silica-coated product is prepared. In order to analyse the morphology, colloidal stability, and surface properties of these two types of coated particles, a detailed study by means of TEM, DLS, zeta-potential measurements, and IR spectroscopy is carried out. The experiments on the titania-coated sample reveal a continuous though porous character of the TiO2 shell. Finally, the relaxometric study at the magnetic field of 0.5 T, performed to quantity the transverse relaxivity and its temperature dependence, reveals important differences between the titania-coated and silica-coated nanoparticles. Pracoviště Fyzikální ústav Kontakt Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Rok sběru 2018
Počet záznamů: 1