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Is it possible to measure diameters of metal nanoparticles using BSE imaging in FESEM?
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SYSNO ASEP 0397203 Druh ASEP J - Článek v odborném periodiku Zařazení RIV J - Článek v odborném periodiku Poddruh J Článek ve WOS Název Is it possible to measure diameters of metal nanoparticles using BSE imaging in FESEM? Tvůrce(i) Nebesářová, Jana (BC-A) RID, ORCID
Langhans, Jan (BC-A)
Šlouf, Miroslav (UMCH-V) RID, ORCID
Pavlova, Ewa (UMCH-V) RID
Vancová, Marie (BC-A) RID, ORCIDZdroj.dok. Micron. - : Elsevier - ISSN 0968-4328
Roč. 44, JAN 2013 (2013), s. 159-166Poč.str. 8 s. Forma vydání Tištěná - P Jazyk dok. eng - angličtina Země vyd. GB - Velká Británie Klíč. slova Au nanoparticles ; Autrata YAG detector of BSE signal ; FESEM ; Pd nanoparticles ; Size measurement Vědní obor RIV EA - Morfologické obory a cytologie CEP KAN200520704 GA AV ČR - Akademie věd GAP205/10/0348 GA ČR - Grantová agentura ČR Institucionální podpora BC-A - RVO:60077344 ; UMCH-V - RVO:61389013 UT WOS 000312925300015 DOI 10.1016/j.micron.2012.06.002 Anotace The possibilities of using a field emission scanning electron microscope (FESEM) equipped with an Autrata improved yttrium aluminum garnet (YAG) detector of back-scattered electrons (BSE) for a determination of metal nanoparticles sizes were examined in this study. The diameters of Au and Pd nanoparticles with different sizes were resolved based on digitally recorded FESEM micrographs and were compared with diameters obtained with a transmission electron microscope (TEM). In the case of Au nanoparticles, the data obtained from the FESEM exhibited smaller values in comparison with data from the TEM. The Pd nanoparticles diameters measured in the FESEM were comparable with those determined by means of the TEM, however. The influence of various parameters like the sizes of nanoparticles, their composition, use of accelerating voltage and other working conditions in the FESEM on the measurement results are discussed. Pracoviště Biologické centrum (od r. 2006) Kontakt Dana Hypšová, eje@eje.cz, Tel.: 387 775 214 Rok sběru 2014
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