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Polymeric nanoparticles stabilized by surfactants investigated by light scattering, small-angle neutron scattering, and Cryo-TEM methods
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SYSNO ASEP 0359807 Druh ASEP J - Článek v odborném periodiku Zařazení RIV J - Článek v odborném periodiku Poddruh J Článek ve WOS Název Polymeric nanoparticles stabilized by surfactants investigated by light scattering, small-angle neutron scattering, and Cryo-TEM methods Tvůrce(i) Pánek, Jiří (UMCH-V) RID, ORCID
Filippov, Sergey K. (UMCH-V) RID, ORCID, SAI
Koňák, Čestmír (UMCH-V) RID
Nallet, F. (FR)
Noirez, L. (FR)
Karlsson, G. (SE)
Štěpánek, Petr (UMCH-V) RID, ORCIDZdroj.dok. Journal of Dispersion Science and Technology - ISSN 0193-2691
Roč. 32, č. 6 (2011), s. 888-897Poč.str. 10 s. Jazyk dok. eng - angličtina Země vyd. US - Spojené státy americké Klíč. slova Cryo-TEM ; DLS ; nanoparticles Vědní obor RIV BO - Biofyzika CEP GA202/09/2078 GA ČR - Grantová agentura ČR CEZ AV0Z40500505 - UMCH-V (2005-2011) UT WOS 000290988400018 DOI https://doi.org/10.1080/01932691.2010.488475 Anotace We investigated self-organization of polymers with surfactants through solvent shifting process resulting in formation of stable and uniform nanoparticles. We studied polymeric nanoparticles made of poly(methylmethacrylate) and of polystyrene dispersed in water. We observed the formation of well defined nanoparticles by light scattering, small-angle neutron scattering (SANS), and cryogenic transmission electron microscopy (Cryo-TEM) methods. The study shows how nanoparticle properties are changed by the chemical composition of surfactants, molar mass of polymers, concentrations of both components. Dynamic light scattering (DLS) and static light scattering (SLS) provide the hydrodynamic radii and radii of gyration, cryo-TEM experiments prove that the nanoparticles have good spherical shape. Analysis of SANS data and cryo-TEM micrographs suggest that the prepared particles are composed of polymer and surfactant that are evenly distributed. Pracoviště Ústav makromolekulární chemie Kontakt Eva Čechová, cechova@imc.cas.cz ; Tel.: 296 809 358 Rok sběru 2012
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