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Reciprocal and real space maps for EMCD experiments
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SYSNO ASEP 0357422 Druh ASEP J - Článek v odborném periodiku Zařazení RIV J - Článek v odborném periodiku Poddruh J Článek ve WOS Název Reciprocal and real space maps for EMCD experiments Tvůrce(i) Lidbaum, H. (SE)
Rusz, Ján (FZU-D)
Rubino, S. (SE)
Liebig, A. (SE)
Hjörvarsson, B. (SE)
Oppeneer, P.M. (SE)
Eriksson, A. (SE)
Leifer, K. (SE)Zdroj.dok. Ultramicroscopy. - : Elsevier - ISSN 0304-3991
Roč. 110, č. 11 (2010), s. 1380-1389Poč.str. 10 s. Jazyk dok. eng - angličtina Země vyd. NL - Nizozemsko Klíč. slova magnetic circular dichroism ; electron energy-loss spectra ; transmission electron microscopy Vědní obor RIV BM - Fyzika pevných látek a magnetismus CEZ AV0Z10100520 - FZU-D (2005-2011) UT WOS 000282562100005 DOI 10.1016/j.ultramic.2010.07.004 Anotace Electron magnetic chiral dichroism (EMCD) is an emerging tool for quantitative measurements of magnetic properties using the transmission electron microscope (TEM), with the possibility of nanometer resolution. The geometrical conditions, data treatment and electron gun settings are found to influence the EMCD signal. In this article, particular care is taken to obtain a reliable quantitative measurement of the ratio of orbital to spin magnetic moment using energy filtered diffraction patterns. We describe a method for data treatment, normalization and selection of mirror axis. The experimental results are supported by theoretical simulations based on dynamical diffraction and density functional theory. Using special settings, we demonstrate the principle of acquiring real space maps of the EMCD signal. This enables advanced characterization of magnetic materials with superior spatial resolution. Pracoviště Fyzikální ústav Kontakt Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Rok sběru 2011
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