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Effect of sonication on phase transfer catalysis reaction in continuous flow synthesis
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SYSNO ASEP 0598064 Druh ASEP A - Abstrakt Zařazení RIV Záznam nebyl označen do RIV Zařazení RIV Není vybrán druh dokumentu Název Effect of sonication on phase transfer catalysis reaction in continuous flow synthesis Tvůrce(i) Jaklová, Natalie (UCHP-M) SAI
Stavárek, Petr (UCHP-M) RID, ORCID, SAI
Vychodilová, Hana (UCHP-M) RID, SAI
Malíková, S. (CZ)
Salmi, T. (FI)
Klusoň, Petr (UCHP-M) RID, ORCID, SAIČíslo článku 0370 Zdroj.dok. Author Index. - Prague : Czech Society of Chemical Engineering, 2024
C1.4Poč.str. 2 s. Forma vydání Online - E Akce International Congress of Chemical and Process Engineering CHISA 2024 /27./ Datum konání 25.08.2024 - 29.08.2024 Místo konání Prague Země CZ - Česká republika Typ akce EUR Jazyk dok. eng - angličtina Země vyd. CZ - Česká republika Klíč. slova catalysis reaction ; flow synthesis ; sonification Obor OECD Chemical process engineering Institucionální podpora UCHP-M - RVO:67985858 Anotace Based on the collected results, a new objective was set to verify the possibility of applying the obtained knowledge during the study of PTC reactions and ultrasound effects to another type of PTC N-alkylation. The intention was thus to develop general approaches for the continuation and intensification of organic syntheses containing PCT reactions. In contrast to previously studied N-alkylation with liquid-liquid phase system, the newly chosen N-alkylation reaction is carried out at the solid-liquid interface. The hypothesis for the solid-liquid arrangement is that sonication accelerates transport from the surface of the solid phase to the organic phase and thus intensify the reaction. The continuous reactor adjustments to accommodate for the solid phase as well as effect of sonication on the course of the N-alkylation reaction will be provided and discussed based on the experimental results. Pracoviště Ústav chemických procesů Kontakt Eva Jirsová, jirsova@icpf.cas.cz, Tel.: 220 390 227 Rok sběru 2025
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