Influence of purity and grain size distribution of powdered NaCl on its thermal properties

0581873 - FZÚ 2024 RIV HU eng A - Abstrakt
Falvey, Alexandra - Král, Robert - Zemenová, Petra - Vaněček, Vojtěch - Stehlík, Štěpán
Influence of purity and grain size distribution of powdered NaCl on its thermal properties.
Book of Abstracts JTACC + V4 (2023). Budapest: Akadémiai Kiadó / AKCongress, 2023. s. 296-297. ISBN 978-963-454-915-4.
[Journal of Thermal Analysis and Calorimetry Conference /3./ and V4 /9./. 20.06.2023-23.06.2023, Balatonfüred]
Grant CEP: GA TA ČR(CZ) FW06010047
Institucionální podpora: RVO:68378271
Klíčová slova: thermal analysis * NaCl * particle size * purity * moisture content
Obor OECD: Inorganic and nuclear chemistry
https://static.akcongress.com/downloads/jtacc/jtacc2023-book-of-abstracts.pdf

The aim of this work is to study NaCl samples using thermal analyses in the powder form and single crystal NaCl ingot and to describe the processes that occur in the samples during their thermal treatment. Further, the effect of grain size in NaCl powder samples, the effect of purity and moisture content on its behavior under thermal treatment was characterized. The samples were studied by thermal analyses including non-isothermal differential scanning calorimetry (DSC), thermogravimetry (TGA), thermomechanical analysis (TMA), mass spectrometry (MS), and optical stereomicroscopy (OM). The TMA showed that the smaller the grain size, the earlier the grains are densified and subsequently sintered when heated. On the other hand, the influence of NaCl powder grain size distribution on the course of the TMA curves was recorded and showed a significant influence on the sintering effect.

Trvalý link: https://hdl.handle.net/11104/0350007