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Incommensurately modulated structures in Pb(Zr.sub.1-x./sub.Sn.sub.x./sub.)O.sub.3./sub. single crystals by x-ray diffraction

  1. 1.
    0547452 - FZÚ 2022 RIV US eng J - Článek v odborném periodiku
    Jankowska-Sumara, I. - Pasciak, Marek - Podgorna, M. - Majchrowski, A. - Kopecký, Miloš - Kub, Jiří
    Incommensurately modulated structures in Pb(Zr1-xSnx)O3 single crystals by x-ray diffraction.
    APL Materials. Roč. 9, č. 2 (2021), č. článku 021101. ISSN 2166-532X. E-ISSN 2166-532X
    Grant CEP: GA MŠMT(CZ) EF16_019/0000760
    Grant ostatní: OP VVV - SOLID21(XE) CZ.02.1.01/0.0/0.0/16_019/0000760; AV ČR(CZ) StrategieAV21/3
    Program: StrategieAV
    Institucionální podpora: RVO:68378271
    Klíčová slova: incommensurate structures * antiferroelectrics * disorder
    Obor OECD: Condensed matter physics (including formerly solid state physics, supercond.)
    Impakt faktor: 6.635, rok: 2021
    Způsob publikování: Open access

    Pb(Zr1−xSnx)O3 single crystals were characterized using x-ray diffraction as a function of temperature and composition. The information on the structure of two intermediate phases, situated between antiferroelectric and paraelectric phases in the composition–temperature phase diagram, has been obtained. The lower-temperature intermediate phase is characterized by incommensurate displacive modulations in the Pb sublattice. The higher temperature intermediate phase is characterized by distortions of the oxygen sublattice primarily in the form of anti-phase tilts of the oxygen octahedra. The structured diffuse scattering was also observed in the paraelectric phase along Γ–M and M–R lines pointing to the high-temperature correlated disorder of Pb ions and octahedral rotations, respectively.
    Trvalý link: http://hdl.handle.net/11104/0323890

     
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