On Shear Testing of Single Crystal Ni-Base Superalloys

0496505 - ÚFM 2019 RIV US eng J - Článek v odborném periodiku
Eggeler, G. - Wieczorek, N. - Fox, F. - Berglund, S. - Bürger, D. - Dlouhý, Antonín - Wollgramm, P. - Neuking, K. - Schreuer, J. - Jácome, L. A. - Gao, S. - Hartmaier, A. - Laplanche, G.
On Shear Testing of Single Crystal Ni-Base Superalloys.
Metallurgical and Materials Transactions A. Roč. 49A, č. 9 (2018), s. 3951-3962. ISSN 1073-5623. E-ISSN 1543-1940
Grant CEP: GA MŠMT(CZ) LQ1601
Institucionální podpora: RVO:68081723
Klíčová slova: high-temperature creep * nickel-based superalloys * microstructure
Obor OECD: Materials engineering
Impakt faktor: 1.985, rok: 2018

Shear testing can contribute to a better understanding of the plastic deformation of Ni-base superalloy single crystals. In the present study, shear testing is discussed with special emphasis placed on its strengths and weaknesses. Key mechanical and microstructural results which were obtained for the high-temperature (T ≈ 1000 °C) and low-stress (τ ≈ 200 MPa) creep regime are briefly reviewed. New 3D stereo STEM images of dislocation substructures which form during shear creep deformation in this regime are presented. It is then shown which new aspects need to be considered when performing double shear creep testing at lower temperatures (T < 800 °C) and higher stresses (τ > 600 MPa). In this creep regime, the macroscopic crystallographic [11−2](111) shear system deforms significantly faster than the [01−1](111) system. This represents direct mechanical evidence for a new planar fault nucleation scenario, which was recently suggested (Wu et al. in Acta Mater 144:642–655, 2018). The double shear creep specimen geometry inspired a micro-mechanical in-situ shear test specimen. Moreover, the in-situ SEM shear specimen can be FIB micro-machined from prior dendritic and interdendritic regions. Dendritic regions, which have a lower γ′ volume fraction, show a lower critical resolved shear stress.
Trvalý link: http://hdl.handle.net/11104/0289277