Počet záznamů: 1
Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta
- 1.0399810 - ÚOCHB 2014 RIV GB eng J - Článek v odborném periodiku
Hrubá, L. - Buděšínský, Miloš - Pícha, Jan - Jiráček, Jiří - Vaněk, Václav
Simplified syntheses of the water-soluble chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta.
Tetrahedron Letters. Roč. 54, č. 47 (2013), s. 6296-6297. ISSN 0040-4039. E-ISSN 1873-3581
Institucionální podpora: RVO:61388963
Klíčová slova: NMR * chiral shift reagents * Sm-pdta * PDTA * samarium * 1,2-diaminopropane
Kód oboru RIV: CC - Organická chemie
Impakt faktor: 2.391, rok: 2013
The chiral shift reagents Sm-(R)-pdta and Sm-(S)-pdta, which are based on (R)- or (S)-1,2-diaminopropane-N,N,N',N'-tetraacetic acid were synthesized from easily accessible compounds in three simple steps, which makes the method suitable for laboratory-scale production. In addition, a new and efficient method for the preparation of pure anhydrous (R)- or (S)-1,2-diaminopropane-N,N,N',N'-tetraacetic acid was developed.
Trvalý link: http://hdl.handle.net/11104/0227147
Počet záznamů: 1