NMR spectroscopy and atomic force microscopy characterization of hybrid organic ů inorganic coatings

0189068 - UMCH-V 20033021 RIV DE eng C - Konferenční příspěvek (zahraniční konf.)
Špírková, Milena - Brus, Jiří
NMR spectroscopy and atomic force microscopy characterization of hybrid organic ů inorganic coatings.
Congress Papers. Nürnberg: International Centre for Coatings Technology, 2003, s. 312-324. 1. ISBN 3-87870-145-4.
[Nürnberg Congress: Creative Advances in Coatings Technology /7./. Nürnberg (DE), 07.04.2003-08.04.2003]
Grant CEP: GA ČR GA203/01/0735; GA ČR GA203/98/P290; GA AV ČR IAA4050008
Výzkumný záměr: CEZ:AV0Z4050913
Klíčová slova: coatings and films * sol-gel process * NMR spectroscopy
Kód oboru RIV: CD - Makromolekulární chemie

Hybrid organicůinorganic epoxide-based products made from functionalized organosilica precursors, oligomeric di- and triamines and, in some cases, colloidal silica particles were characterized. The structure development (kinetics and reaction mechanism of condensation reactions), structure and segmental dynamics of final films, as well as homogeneity were studied by NMR spectroscopy (2D CRAMPS, 2D 1H-13C WISE, relaxation experiments, etc.); the surface morphology and other surface characteristics were determined by atomic force microscopy.
Trvalý link: http://hdl.handle.net/11104/0084923