Počet záznamů: 1

Synthesis, characterization and crystal structure of N,N'-Bis(2,3-Dimethoxybenzylidene)-1,2-Diaminoethane

  1. 1.
    0369331 - FZU-D 2012 RIV US eng J - Článek v odborném periodiku
    Khalaji, A.D. - Fejfarová, Karla - Dušek, Michal - Bijanzadeh, H.R.
    Synthesis, characterization and crystal structure of N,N'-Bis(2,3-Dimethoxybenzylidene)-1,2-Diaminoethane.
    Journal of Chemical Crystallography. Roč. 41, č. 12 (2011), 1955-1960 ISSN 1074-1542
    Výzkumný záměr: CEZ:AV0Z10100521
    Klíčová slova: Shiff bases * X-ray diffraction * Jana2006 * crystal structure * characterization
    Kód oboru RIV: BM - Fyzika pevných látek a magnetismus
    Impakt faktor: 0.566, rok: 2011

    Synthesis and characterization of single crystals of a new organic Schiff-base derivative, N,N'-bis(2,3-dimethoxybenzylidene)-1,2-diaminoethane is reported. Good quality single crystals with size 10 mm x 1 mm x 1 mm were grown by slow evaporation technique from a methanol solution at room temperature. The grown crystals have been characterized by elemental analyses and functional groups were identified using FT-IR and 1H-NMR spectroscopy. Crystal structure of the title compound has been determined by single crystal X-ray diffraction. The title compound has a monoclinic symmetry, space group P21/c, lattice parameters are a = 4.4159(3) A, b = 14.2333(9) A, c = 15.0601(10) A, beta = 97.755(5)°, Z = 2, V = 937.91(11) A3.
    Trvalý link: http://hdl.handle.net/11104/0203424