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One-step Preparation of Antimicrobial Silver Nanoparticles in Polymer Matrix.
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SYSNO ASEP 0443173 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title One-step Preparation of Antimicrobial Silver Nanoparticles in Polymer Matrix. Author(s) Lyutakov, O. (CZ)
Kalachyova, Y. (CZ)
Solovyev, Andrey (UCHP-M) RID, ORCID, SAI
Vytykačová, S. (CZ)
Švanda, J. (CZ)
Siegel, J. (CZ)
Ulbrich, P. (CZ)
Švorčík, V. (CZ)Source Title Journal of Nanoparticle Research. - : Springer - ISSN 1388-0764
Roč. 17, č. 3 (2015), s. 120Number of pages 11 s. Language eng - English Country NL - Netherlands Keywords polymer ; silver nanoparticles ; antimicrobial test Subject RIV JJ - Other Materials R&D Projects GBP108/12/G108 GA ČR - Czech Science Foundation (CSF) Institutional support UCHP-M - RVO:67985858 UT WOS 000355016500001 EID SCOPUS 84924405796 DOI https://doi.org/10.1007/s11051-015-2935-3 Annotation Simple one-step procedure for in situ preparation of silver nanoparticles (AgNPs) in the polymer thin films is described. Nanoparticles (NPs) were prepared by reaction of N-methyl pyrrolidone with silver salt in semi-dry polymer film and characterized by transmission electron microscopy, XPS, and UV–Vis spectroscopy techniques. Direct synthesis of NPs in polymer has several advantages; even though it avoids time-consuming NPs mixing with polymer matrix, uniform silver distribution in polymethylmethacrylate (PMMA) films is achieved without necessity of additional stabilization. The influence of the silver concentration, reaction temperature and time on reaction conversion rate, and the size and size-distribution of the AgNPs was investigated. Polymer films doped with AgNPs were tested for their antibacterial activity on Gram-negative bacteria. Antimicrobial properties of AgNPs/PMMA films were found to be depended on NPs concentration, their size and distribution. Proposed one-step synthesis of functional polymer containing AgNPs is environmentally friendly, experimentally simple and extremely quick. It opens up new possibilities in development of antimicrobial coatings with medical and sanitation applications. Workplace Institute of Chemical Process Fundamentals Contact Eva Jirsová, jirsova@icpf.cas.cz, Tel.: 220 390 227 Year of Publishing 2016
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