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Evolution of carbon and oxygen concentration in tungsten prepared by field assisted sintering and its effect on ductility

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    SYSNO ASEP0542799
    Document TypeJ - Journal Article
    R&D Document TypeJournal Article
    Subsidiary JČlánek ve WOS
    TitleEvolution of carbon and oxygen concentration in tungsten prepared by field assisted sintering and its effect on ductility
    Author(s) Veverka, Jakub (UFP-V) ORCID
    Vilémová, Monika (UFP-V) RID, ORCID
    Chlup, Zdeněk (UFM-A) RID, ORCID
    Hadraba, Hynek (UFM-A) RID, ORCID
    Lukáč, František (UFP-V) ORCID
    Csáki, Štefan (UFP-V) ORCID
    Matějíček, Jiří (UFP-V) RID, ORCID
    Vontorová, J. (CZ)
    Chráska, Tomáš (UFP-V) RID, ORCID
    Number of authors9
    Article number105499
    Source TitleInternational Journal of Refractory Metals & Hard Materials. - : Elsevier - ISSN 0263-4368
    Roč. 97, June (2021)
    Number of pages12 s.
    Languageeng - English
    CountryNL - Netherlands
    KeywordsCarbon concentration ; Ductile behaviour ; Oxygen concentration ; Sintering atmosphere ; Sintering foil ; Spark plasma sintering ; Stress-strain ; Tungsten
    Subject RIVJG - Metallurgy
    OECD categoryMaterials engineering
    Subject RIV - cooperationInstitute of Physics of Materials - Materials Fatigue, Friction Mechanics
    R&D ProjectsGA20-18392S GA ČR - Czech Science Foundation (CSF)
    Method of publishingLimited access
    Institutional supportUFP-V - RVO:61389021 ; UFM-A - RVO:68081723
    UT WOS000638214500011
    EID SCOPUS85100907090
    DOI10.1016/j.ijrmhm.2021.105499
    AnnotationGood thermal conductivity, high-temperature strength and low tritium retention favour the use of tungsten as a plasma facing material for fusion reactors. However, high ductile-to-brittle transition temperature (DBTT) of tungsten limits its application. The most viable way of industrial-scale tungsten production is powder metallurgy. Conventional methods use high temperatures and long dwell times. However, this can degrade the mechanical properties of tungsten due to excessive grain growth. Therefore, new sintering techniques and unconventional sintering parameters are explored. The aim is to achieve less demanding single step processing method with the potential to improve mechanical properties. In this study, pure tungsten samples were prepared by Field Assisted Sintering using different dwell times, atmospheres and foils. The effect of the parameters on the impurity concentration was analysed and the mechanical behaviour was evaluated using stress-strain analysis. Significant improvement in mechanical performance has been reached for short dwell times (2 min) and vacuum or Ar + H atmosphere. 2
    WorkplaceInstitute of Plasma Physics
    ContactVladimíra Kebza, kebza@ipp.cas.cz, Tel.: 266 052 975
    Year of Publishing2022
    Electronic addresshttps://www.sciencedirect.com/science/article/pii/S0263436821000317?via%3Dihub
Number of the records: 1  

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