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3D electron diffraction: the nanocrystallography revolution

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    SYSNO ASEP0522225
    Document TypeJ - Journal Article
    R&D Document TypeJournal Article
    Subsidiary JČlánek ve WOS
    Title3D electron diffraction: the nanocrystallography revolution
    Author(s) Gemmi, M. (IT)
    Mugnaioli, E. (IT)
    Gorelik, T.E. (DE)
    Kolb, U. (DE)
    Palatinus, Lukáš (FZU-D) RID, ORCID
    Boullay, P. (FR)
    Hovmoller, S. (SE)
    Abrahams, J.P. (CH)
    Number of authors8
    Source TitleACS Central Science. - : American Chemical Society - ISSN 2374-7943
    Roč. 5, č. 8 (2019), s. 1315-1329
    Number of pages14 s.
    Languageeng - English
    CountryUS - United States
    Keywordsnanocrystalline materials ; electron diffraction ; 3D acquisition ; crystal structure
    Subject RIVBM - Solid Matter Physics ; Magnetism
    OECD categoryCondensed matter physics (including formerly solid state physics, supercond.)
    Method of publishingOpen access
    Institutional supportFZU-D - RVO:68378271
    UT WOS000486591500007
    EID SCOPUS85075945528
    DOI10.1021/acscentsci.9b00394
    AnnotationCrystallography of nanocrystalline materials has witnessed a true revolution in the past 10 years, thanks to the introduction of protocols for 3D acquisition and analysis of electron diffraction data. This method provides single-crystal data of structure solution and refinement quality, allowing the atomic structure determination of those materials that remained hitherto unknown because of their limited crystallinity. Several experimental protocols exist, which share the common idea of sampling a sequence of diffraction patterns while the crystal is tilted around a noncrystallographic axis, namely, the goniometer axis of the transmission electron microscope sample stage. This Outlook reviews most important 3D electron diffraction applications for different kinds of samples and problematics, related with both materials and life sciences. Structure refinement including dynamical scattering is also briefly discussed.
    WorkplaceInstitute of Physics
    ContactKristina Potocká, potocka@fzu.cz, Tel.: 220 318 579
    Year of Publishing2020
    Electronic addresshttp://hdl.handle.net/11104/0306743
Number of the records: 1  

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