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X-ray Computed Tomographic Investigation of the Porosity and Morphology of Plasma Electrolytic Oxidation Coatings

  1. 1.
    SYSNO ASEP0465628
    Document TypeJ - Journal Article
    R&D Document TypeJournal Article
    Subsidiary JČlánek ve WOS
    TitleX-ray Computed Tomographic Investigation of the Porosity and Morphology of Plasma Electrolytic Oxidation Coatings
    Author(s) Zhang, X. (GB)
    Aliasghari, S. (GB)
    Němcová, A. (GB)
    Burnett, T.L. (GB)
    Kuběna, Ivo (UFM-A) RID, ORCID
    Šmíd, Miroslav (UFM-A) RID, ORCID
    Thompson, G. (GB)
    Skeldon, P. (GB)
    Withers, P.J. (GB)
    Number of authors9
    Source TitleACS Applied Materials and Interfaces. - : American Chemical Society - ISSN 1944-8244
    Roč. 8, č. 13 (2016), s. 8801-8810
    Number of pages10 s.
    Languageeng - English
    CountryUS - United States
    Keywordsplasma electrolytic oxidation ; porosity ; scanning electron microscopy ; titanium ; X-ray computed tomography
    Subject RIVJK - Corrosion ; Surface Treatment of Materials
    R&D ProjectsED1.1.00/02.0068 GA MŠMT - Ministry of Education, Youth and Sports (MEYS)
    Institutional supportUFM-A - RVO:68081723
    UT WOS000373748200058
    EID SCOPUS84964522879
    DOI10.1021/acsami.6b00274
    AnnotationPlasma electrolytic oxidation (PEO) is of increasing interest for the formation of ceramic coatings on metals for applications that require diverse coating properties, such as wear and corrosion resistance, low thermal conductivity, and biocompatibility. Porosity in the coatings can have an important impact on the coating performance. However, the quantification of the porosity in coatings can be difficult due to the wide range of pore sizes and the complexity of the coating morphology. In this work, a PEO coating formed on titanium is examined using high resolution X-ray computed tomography (X-ray CT). The observations are validated by comparisons of surface views and cross-sectional views of specific coating features obtained using X-ray CT and scanning electron microscopy. The X-ray CT technique is shown to be capable of resolving pores with volumes of at least 6 μm3. Furthermore, the shapes of large pores are revealed and a correlation is demonstrated between the locations of the pores, nodules on the coating surface, and depressions in the titanium substrate. The locations and morphologies of the pores, which constitute 5.7% of the coating volume, indicate that they are generated by release of oxygen gas from the molten coating.
    WorkplaceInstitute of Physics of Materials
    ContactYvonna Šrámková, sramkova@ipm.cz, Tel.: 532 290 485
    Year of Publishing2017
Number of the records: 1  

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