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Filamentation of diamond nanoparticles treated in underwater corona discharge
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SYSNO ASEP 0458854 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Filamentation of diamond nanoparticles treated in underwater corona discharge Author(s) Jirásek, Vít (FZU-D) RID
Lukeš, Petr (UFP-V) RID, ORCID
Kozak, Halyna (FZU-D) RID, ORCID
Artemenko, Anna (FZU-D) RID, ORCID
Člupek, Martin (UFP-V) RID
Čermák, Jan (FZU-D) RID, SAI, ORCID
Rezek, Bohuslav (FZU-D) RID, ORCID
Kromka, Alexander (FZU-D) RID, ORCID, SAISource Title RSC Advances. - : Royal Society of Chemistry
Roč. 6, č. 3 (2016), 2352-2360Number of pages 9 s. Language eng - English Country GB - United Kingdom Keywords nanodiamonds ; pulsed streamer corona discharge ; filamentation Subject RIV BM - Solid Matter Physics ; Magnetism R&D Projects GA15-01687S GA ČR - Czech Science Foundation (CSF) LD14011 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) Institutional support FZU-D - RVO:68378271 ; UFP-V - RVO:61389021 UT WOS 000368191100079 EID SCOPUS 84954094158 DOI 10.1039/c5ra23292a Annotation Diamond nanoparticles (DNPs) with a nominal diameter of 5 nm were treated using underwater pulsed streamer corona discharge. A reactor with a needle-to-plate electrode system was employed. The electrolytic conductivity of aqueous DNPs suspensions (0.37 g l-1) was adjusted by NaCl to 100 and 500 mS cm-1. The discharge-treated particles predominantly formed several mm long filaments consisting of agglomerates with submicron diameter, independent of the solution conductivity and the treatment time. The treatment of DNPs decreased the sp2-bonded carbon atoms, as evaluated by XPS for more conductive solution. For both solutions, oxidation of the DNP surface was observed. FTIR measurements showed evolution of new bands at 800–950 cm-1 and 1261 cm-1, which were attributed to the formation of epoxides via the attack of HO2 radicals on surface C=C double bonds. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2017
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