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Characterization and crystal structures of new Schiff base macrocyclic compounds

SYSNO ASEP	0456817
Document Type	J - Journal Article
R&D Document Type	Journal Article
Subsidiary J	Článek ve WOS
Title	Characterization and crystal structures of new Schiff base macrocyclic compounds
Author(s)	Khalaji, A.D. (IR) Ghoran, S.H. (IR) Pojarová, Michaela (FZU-D)_{RID, ORCID} Dušek, Michal (FZU-D)_{RID, ORCID, SAI}
Source Title	Journal of Structural Chemistry. - : Pleiades Publishing - ISSN 0022-4766 Roč. 56, č. 7 (2015), s. 1410-1414
Number of pages	5 s.
Language	eng - English
Country	RU - Russian Federation
Keywords	synthesis ; macrocyclic Schiff base ; single crystal structure analysis ; spectroscopy
Subject RIV	BM - Solid Matter Physics ; Magnetism
R&D Projects	GA14-03276S GA ČR - Czech Science Foundation (CSF)
Institutional support	FZU-D - RVO:68378271
UT WOS	000369060300024
DOI	10.1134/S0022476615070240
Annotation	We report the synthesis and characterization of two new macrocyclic Schiff base compounds: a 15-membered (1) and 16-membered (2) one. Their synthesis involves a Schiff base condensation of 2,2-dimethylpropanediamine and two dialdehydes: 5,5′-dimethoxy-2,2′-(ethane-1,2-diyldioxy)dibenzaldehyde and 5,5′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzaldehyde. The compounds are characterized by elemental analysis (CHN), FT-IR, 1H and 13C-NMR spectroscopy, and single crystal X-ray diffraction.
Workplace	Institute of Physics
Contact	Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579
Year of Publishing	2016

Number of the records: 1