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Characterisation and development of fine porosity in magnesium potassium phosphate ceramics
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SYSNO ASEP 0452457 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Characterisation and development of fine porosity in magnesium potassium phosphate ceramics Author(s) Viani, Alberto (UTAM-F) RID, ORCID, SAI
Radulescu, A. (DE)
Pérez-Estébanez, Marta (UTAM-F) RID, SAINumber of authors 3 Source Title Materials Letters. - : ELSEVIER SCIENCE BV - ISSN 0167-577X
Roč. 161, December (2015), s. 628-630Number of pages 3 s. Publication form Print - P Language eng - English Country NL - Netherlands Keywords amorphous materials ; chemically-bonded ceramics ; microstructure ; Rietveld-RIR method ; small-angle neutron scattering ; specific surface area Subject RIV AL - Art, Architecture, Cultural Heritage R&D Projects LO1219 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) UT WOS 000364891700162 EID SCOPUS 84942251698 DOI 10.1016/j.matlet.2015.09.056 Annotation Characterisation of porosity and microstructure in chemically-bonded ceramics was accomplished by small-angle neutron scattering. Microstructural parameters were also followed during the setting reaction and obtained kinetic curves were compared with results of XRD quantitative phase analysis up to 1 month. Results indicate that less reactive MgO yields a more compact microstructure, the same happens during the progress of the reaction. The reaction product forms from an amorphous precursor and its development was found to scale with the microstructural parameters. A change in reaction mechanism after 40 min is suggested. Workplace Institute of Theoretical and Applied Mechanics Contact Kulawiecová Kateřina, kulawiecova@itam.cas.cz, Tel.: 225 443 285 Year of Publishing 2016
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