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Annual Reports on NMR Spectroscopy
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SYSNO ASEP 0428780 Document Type M - Monograph Chapter R&D Document Type Monograph Chapter Title NMR Studies of Purines Author(s) Dračínský, Martin (UOCHB-X) RID, ORCID
Pohl, Radek (UOCHB-X) RID, ORCIDNumber of authors 2 Source Title Annual Reports on NMR Spectroscopy, 82. - Oxford : Academic Press, 2014 / Webb G. A. - ISBN 978-0-12-800184-4 Pages s. 59-113 Number of pages 55 s. Number of pages 257 Publication form Print - P Language eng - English Country GB - United Kingdom Keywords NMR spectroscopy ; purines ; DFT calculations ; chemical shifts Subject RIV CC - Organic Chemistry R&D Projects GA13-24880S GA ČR - Czech Science Foundation (CSF) Institutional support UOCHB-X - RVO:61388963 UT WOS 000348704700003 EID SCOPUS 84899584328 DOI 10.1016/B978-0-12-800184-4.00002-3 Annotation The experimental NMR methods and theoretical calculations of NMR parameters used in the studies of purine derivatives are reviewed. The first part of this chapter brings an overview of the experimental techniques that are commonly used for hydrogen, carbon and nitrogen NMR signal detection and assignment, followed by a detailed discussion of the influence of purine substitution on NMR parameters. The applications of solid-state NMR methods and the calculations of chemical shifts and indirect coupling constants of purines are also reviewed. The second part of this chapter summarises recent applications (since 2005) of these techniques in the studies of purine structure and interactions. Workplace Institute of Organic Chemistry and Biochemistry Contact asep@uochb.cas.cz ; Kateřina Šperková, Tel.: 232 002 584 ; Viktorie Chládková, Tel.: 232 002 434 Year of Publishing 2015
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