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Synthesis and characterization of Sn-rich Ni-Sb-Sn nanosolders
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SYSNO ASEP 0369871 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Synthesis and characterization of Sn-rich Ni-Sb-Sn nanosolders Author(s) Mishra, R. (AT)
Zemanová, Adéla (UFM-A) RID, ORCID
Kroupa, Aleš (UFM-A) RID, ORCID
Flandorfer, H. (AT)
Ipser, H. (AT)Source Title Journal of Alloys and Compounds. - : Elsevier - ISSN 0925-8388
Roč. 513, - (2012), s. 224-229Number of pages 6 s. Language eng - English Country NL - Netherlands Keywords metals and alloys ; nanostructured materials ; nanosolders Subject RIV BJ - Thermodynamics R&D Projects LD11024 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) MEB061005 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) CEZ AV0Z20410507 - UFM-A (2005-2011) UT WOS 000298156400041 DOI 10.1016/j.jallcom.2011.10.023 Annotation Nano-crystalline samples of pure Sn and of Sn-rich ternary Ni-Sb-Sn alloys, with compositions ranging from 80 to 97,5 at% Sn and a Ni to Sb molar ratio of 1:1, were synthesized by reduction of stoichiometric metal chloride solutions with NaBH4 at 0°C in alkaline medium. The melting temperatures of the annealed samples were found to increase progressively with increasing particle size. At the same time, the excess surface energy of these heat treated samples was measured as a function of particle size using a Calvet-type calorimeter. Workplace Institute of Physics of Materials Contact Yvonna Šrámková, sramkova@ipm.cz, Tel.: 532 290 485 Year of Publishing 2012
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