Number of the records: 1
Synthesis, characterization and crystal structure of N,N'-Bis(2,3-Dimethoxybenzylidene)-1,2-Diaminoethane
- 1.
SYSNO ASEP 0369331 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Synthesis, characterization and crystal structure of N,N'-Bis(2,3-Dimethoxybenzylidene)-1,2-Diaminoethane Author(s) Khalaji, A.D. (IR)
Fejfarová, Karla (FZU-D)
Dušek, Michal (FZU-D) RID, ORCID, SAI
Bijanzadeh, H.R. (IR)Source Title Journal of Chemical Crystallography. - : Springer - ISSN 1074-1542
Roč. 41, č. 12 (2011), 1955-1960Number of pages 6 s. Language eng - English Country US - United States Keywords Shiff bases ; X-ray diffraction ; Jana2006 ; crystal structure ; characterization Subject RIV BM - Solid Matter Physics ; Magnetism CEZ AV0Z10100521 - FZU-D (2005-2011) UT WOS 000296883100025 DOI 10.1007/s10870-011-9988-7 Annotation Synthesis and characterization of single crystals of a new organic Schiff-base derivative, N,N'-bis(2,3-dimethoxybenzylidene)-1,2-diaminoethane is reported. Good quality single crystals with size 10 mm x 1 mm x 1 mm were grown by slow evaporation technique from a methanol solution at room temperature. The grown crystals have been characterized by elemental analyses and functional groups were identified using FT-IR and 1H-NMR spectroscopy. Crystal structure of the title compound has been determined by single crystal X-ray diffraction. The title compound has a monoclinic symmetry, space group P21/c, lattice parameters are a = 4.4159(3) A, b = 14.2333(9) A, c = 15.0601(10) A, beta = 97.755(5)°, Z = 2, V = 937.91(11) A3. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2012
Number of the records: 1