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Size-controlled formation of Cu nanoclusters in pulsed magnetron sputtering system
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SYSNO ASEP 0367262 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Size-controlled formation of Cu nanoclusters in pulsed magnetron sputtering system Author(s) Straňák, V. (DE)
Block, S. (DE)
Drache, S. (DE)
Hubička, Zdeněk (FZU-D) RID, ORCID, SAI
Helm, Ch.A. (DE)
Jastrabík, Lubomír (FZU-D) RID, ORCID
Tichý, M. (CZ)
Hippler, R. (DE)Source Title Surface and Coatings Technology. - : Elsevier - ISSN 0257-8972
Roč. 205, 8-9 (2011), s. 2755-2762Number of pages 8 s. Language eng - English Country CH - Switzerland Keywords Cu cluster growth ; pulsed magnetron sputtering ; cluster mass- and size- distribution ; AFM Subject RIV BM - Solid Matter Physics ; Magnetism R&D Projects KAN301370701 GA AV ČR - Academy of Sciences of the Czech Republic (AV ČR) KJB100100805 GA AV ČR - Academy of Sciences of the Czech Republic (AV ČR) 1M06002 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) CEZ AV0Z10100522 - FZU-D (2005-2011) UT WOS 000286905100009 DOI 10.1016/j.surfcoat.2010.10.030 Annotation Size-controlled Cu clusters are formed in a system which combines pulsed magnetron sputtering and gas condensation at room temperature. The discharge repetition frequency (0.1–25 kHz) and the duty cycles (20–90%) of the magnetron sputtering are varied systematically, the influence of discharge current (100–800 mA) and the pressure in the condensation tube (25–90 Pa) is also investigated. For all preparation conditions, the cluster mass shows a lognormal distribution. A non-monotonic frequency dependence with a maximum at 1 kHz and 20% of duty cycle is observed (about 105amu, or cluster diameter 8–10 nm). By adjusting discharge frequency and duty cycle, the cluster mass can be decreased by one order of magnitude. We suggest that this effect is caused by energy dissipated into the aggregation tube; and find a critical buffer gas temperature Tg-cr which limits cluster growth. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2012
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