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Molecular and crystal structure of (E)-4-chloro-N-(3,4-dimethoxybenzylidene)aniline

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    SYSNO ASEP0367190
    Document TypeJ - Journal Article
    R&D Document TypeJournal Article
    Subsidiary JČlánek ve WOS
    TitleMolecular and crystal structure of (E)-4-chloro-N-(3,4-dimethoxybenzylidene)aniline
    Author(s) Khalaji, A.D. (IR)
    Fejfarová, Karla (FZU-D)
    Dušek, Michal (FZU-D) RID, ORCID, SAI
    Source TitleJournal of Structural Chemistry. - : Pleiades Publishing - ISSN 0022-4766
    Roč. 52, č. 4 (2011), s. 835-840
    Number of pages6 s.
    Languageeng - English
    CountryRU - Russian Federation
    KeywordsShiff bases ; crystal structure ; X-ray diffraction
    Subject RIVBM - Solid Matter Physics ; Magnetism
    CEZAV0Z10100521 - FZU-D (2005-2011)
    UT WOS000294824700032
    DOI10.1134/S0022476611040329
    AnnotationThe reaction of 3,4-dimethoxybenzaldehyde with 4-chloroaniline leads to the formation of a new Schiff base (E)-4-chloro-N-(3,4-dimethoxybenzylidene)aniline (1) that is successfully obtained and characterized by elemental analyses, FT-IR and 1H NMR spectroscopy, and single crystal X-ray diffraction. The strong absorption band at 1620 cm–1 in the FT-IR spectrum and a singlet signal at 8.32 ppm in the 1H NMR spectrum of (1) clearly proves the presence of the C=N (azomethine) group. Single crystal X-ray analysis reveals that the title compound adopts an E configuration with respect to the C=N bond.
    WorkplaceInstitute of Physics
    ContactKristina Potocká, potocka@fzu.cz, Tel.: 220 318 579
    Year of Publishing2012
Number of the records: 1  

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