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Synthesis, crystal structure, spectral and thermal studies of (E)-4-dimethamino[(1-phenylethyl)iminomethyl]benzyne
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SYSNO ASEP 0365656 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Synthesis, crystal structure, spectral and thermal studies of (E)-4-dimethamino[(1-phenylethyl)iminomethyl]benzyne Author(s) Khalaji, A.D. (IR)
Rad, S.M. (IR)
Grivani, G. (IR)
Fejfarová, Karla (FZU-D)
Dušek, Michal (FZU-D) RID, ORCID, SAI
Das, D. (IN)Source Title Journal of Chemical Crystallography. - : Springer - ISSN 1074-1542
Roč. 41, č. 8 (2011), s. 1145-1149Number of pages 5 s. Language eng - English Country US - United States Keywords Shiff bases ; crystal structure ; X-ray diffraction Subject RIV BM - Solid Matter Physics ; Magnetism R&D Projects GAP204/11/0809 GA ČR - Czech Science Foundation (CSF) CEZ AV0Z10100521 - FZU-D (2005-2011) UT WOS 000292838900009 DOI 10.1007/s10870-011-0060-4 Annotation Schiff-base compound (E)-4-dimethamino[(1-phenylethyl)iminomethyl]benzyne was synthesized and characterized by elemental analyses (CHN), FT-IR and (1)H-NMR spectroscopic techniques and thermogravimetric analyses (TG). Crystal structure of the title compound was obtained by single crystal X-ray diffraction. The title compound crystallizes in the monoclinic space group P2(1) with unit cell parameters: a = 8.5283(2), b = 6.0699(2), c = 13.6997(4) C(0), beta = 91.471(2)A degrees, V = 708.94(4) C(03) and Z = 2. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2012
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