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Micro/mesoporous conducting carbonized polyaniline 5-sulfosalicylate nanorods/nanotubes: synthesis, characterization and electrocatalysis
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SYSNO ASEP 0365100 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Micro/mesoporous conducting carbonized polyaniline 5-sulfosalicylate nanorods/nanotubes: synthesis, characterization and electrocatalysis Author(s) Janoševic, A. (RS)
Pašti, I. (RS)
Gavrilov, N. (RS)
Mentus, S. (RS)
Ciric-Marjanovic, G. (RS)
Krstic, J. (RS)
Stejskal, Jaroslav (UMCH-V) RID, ORCID, SAISource Title Synthetic Metals. - : Elsevier - ISSN 0379-6779
Roč. 161, 19/20 (2011), s. 2179-2184Number of pages 6 s. Language eng - English Country CH - Switzerland Keywords carbonized polyaniline ; electrocatalysis ; nanorods Subject RIV JI - Composite Materials R&D Projects GA202/09/1626 GA ČR - Czech Science Foundation (CSF) CEZ AV0Z40500505 - UMCH-V (2005-2011) UT WOS 000297182500022 DOI 10.1016/j.synthmet.2011.08.028 Annotation Micro/mesoporous conducting nitrogen-containing carbon nanorods/nanotubes with high surface area, and excellent electrocatalytic activity for the oxygen reduction reaction, were synthesized by the carbonization of self-assembled polyaniline (PANI) 5-sulfosalicylate nanorods/nanotubes. Carbonization was carried out by means of gradual heating in a nitrogen atmosphere up to 800 °C. The morphology, elemental composition, molecular structure, surface area, and electrical characteristics of novel carbonized nanostructured PANI were investigated by scanning and transmission electron microscopies, elemental microanalysis, FTIR and Raman spectroscopies, nitrogen adsorption–desorption and conductivity measurements, respectively. The electrocatalytic activity of carbonized PANI 5-sulfosalicylate nanorods/nanotubes material towards oxygen reduction reaction in alkaline conditions has been studied by the voltammetry with the rotating disc electrode. Workplace Institute of Macromolecular Chemistry Contact Eva Čechová, cechova@imc.cas.cz ; Tel.: 296 809 358 Year of Publishing 2012
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