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The optimized microwave-assisted decomposition of formamides and its synthetic utility in the amination reactions of purines
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SYSNO ASEP 0360741 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title The optimized microwave-assisted decomposition of formamides and its synthetic utility in the amination reactions of purines Author(s) Čechová, Lucie (UOCHB-X) RID, ORCID
Jansa, Petr (UOCHB-X) RID
Šála, Michal (UOCHB-X) RID, ORCID
Dračínský, Martin (UOCHB-X) RID, ORCID
Holý, Antonín (UOCHB-X)
Janeba, Zlatko (UOCHB-X) RID, ORCIDNumber of authors 6 Source Title Tetrahedron. - : Elsevier - ISSN 0040-4020
Roč. 67, č. 5 (2011), s. 866-871Number of pages 6 s. Language eng - English Country GB - United Kingdom Keywords microwave-assisted synthesis ; DMF ; formamides ; dehalogenative amination ; purines Subject RIV CC - Organic Chemistry R&D Projects 1M0508 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) KJB400550903 GA AV ČR - Academy of Sciences of the Czech Republic (AV ČR) CEZ AV0Z40550506 - UOCHB-X (2005-2011) UT WOS 000286995800009 DOI 10.1016/j.tet.2010.12.040 Annotation The microwave-assisted decomposition of DMF was thoroughly studied and the reaction conditions (temperature, solvent effect, and effect of additives such as acids, bases, and salts) were optimized for its use in amination reactions. The applicability of this expedient methodology in purine chemistry and with various formamides is demonstrated. Workplace Institute of Organic Chemistry and Biochemistry Contact asep@uochb.cas.cz ; Kateřina Šperková, Tel.: 232 002 584 ; Viktorie Chládková, Tel.: 232 002 434 Year of Publishing 2012
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