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Non-destructive Depth Profiling of the Activated Ti-Zr-V Getter by Means of Excitation Energy Resolved Photoelectron Spectroscopy
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SYSNO ASEP 0343393 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Non-destructive Depth Profiling of the Activated Ti-Zr-V Getter by Means of Excitation Energy Resolved Photoelectron Spectroscopy Author(s) Pavluch, J. (CZ)
Zommer, L. (PL)
Mašek, K. (CZ)
Skála, T. (IT)
Šutara, F. (CZ)
Nehasil, V. (CZ)
Píš, I. (CZ)
Polyak, Yaroslav (UFCH-W)Source Title Analytical Sciences - ISSN 0910-6340
Roč. 26, č. 2 (2010), s. 209-215Number of pages 7 s. Language eng - English Country JP - Japan Keywords non-evaporable getter materials ; XPS methods Subject RIV CF - Physical ; Theoretical Chemistry CEZ AV0Z40400503 - UFCH-W (2005-2011) UT WOS 000274977700012 EID SCOPUS 77949895185 DOI 10.2116/analsci.26.209 Annotation Non-evaporable Ti-Zr-V ternary getters (NEGs) were studied by means of excitation energy resolved photoelectron spectroscopy (ERXPS). We attempted a quantitative study of the in-depth redistribution of the NEG components during activation. The samples were prepared ex-situ by DC magnetron sputtering on a stainless-steel substrate. The ERXPS measurements were carried out at two incident photoelectron beam angles at energies of 110, 195, 251, 312, 397 and 641 eV. Besides these photon energies, also standard X-ray photoelectron spectroscopy (XPS) was used at a photon energy of 1254 eV. We accumulated Ti 3s, Ti 3p, Ti 3d, V 3s, V 3p, V 3d, Zr 3p, Zr 3d, Zr 4s, Zr 4p, Zr 4d, C 1s, O 1s and O 2s photoelectron peak intensities as functions of the kinetic energies given to them. Under simplifying assumptions, Monte-Carlo calculations of the activated sample concentration profiles were performed to fit the measured spectra intensities. Workplace J. Heyrovsky Institute of Physical Chemistry Contact Michaela Knapová, michaela.knapova@jh-inst.cas.cz, Tel.: 266 053 196 Year of Publishing 2011
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