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Diffusion structural analysis study of titania films deposited by sol-gel technique on silica glass
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SYSNO ASEP 0341374 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Diffusion structural analysis study of titania films deposited by sol-gel technique on silica glass Author(s) Balek, V. (CZ)
Mitsuhashi, T. (JP)
Bountseva, I.M. (RU)
Haneda, H. (JP)
Málek, Z. (CZ)
Šubrt, Jan (UACH-T) SAI, RIDSource Title Journal of Sol-Gel Science and Technology. - : Springer - ISSN 0928-0707
Roč. 26, 1-3 (2003), s. 185-189Number of pages 5 s. Action International Workshop on Glasses, Ceramics, Hybrids and Nanocomposites from Gels /11./ Event date 16.09.2001-21.09.2001 VEvent location Abano Terme Country IT - Italy Event type WRD Language eng - English Country US - United States Keywords titania film ; diffusion structural analysis ; sol-gel Subject RIV CA - Inorganic Chemistry CEZ AV0Z4032918 - UACH-T UT WOS 000178789100032 Annotation The diffusion structural analysis (DSA) was used to characterize microstructure changes of hydrous titania gel films under in situ conditions of heating. TG and DTA were used in order to elucidate the processes controlling the formation of anatase film during heating of hydrous titania gel film. The annealing of porosity and near surface structure defects of the dehydrated titania films was indicated by DSA in the temperature range 255-700degreesC as the decrease of radon release rate. It was demonstrated that the annealing was enhanced on heating in oxygen in comparison with heating in argon. The DSA experimental results were compared with model curves describing the radon diffusion mobility and the annealing of radon diffusion paths. Workplace Institute of Inorganic Chemistry Contact Jana Kroneislová, krone@iic.cas.cz, Tel.: 311 236 931 Year of Publishing 2010
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