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Thermomagnetic Analysis of Nanocrystalline Nd4.5Fe77B18.5 Alloy
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SYSNO ASEP 0339958 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Thermomagnetic Analysis of Nanocrystalline Nd4.5Fe77B18.5 Alloy Author(s) Talijan, N. (CS)
Ćosović, V. (CS)
Stajić-Trošić, J. (CS)
Grujić, A. (CS)
Žák, Tomáš (UFM-A) RID
Lee, Z. (US)
Radmilović, V. (US)Number of authors 7 Source Title Materials Transactions. - : Japan Institute of Metals and Materials - ISSN 1345-9678
Roč. 50, č. 9 (2009), s. 2302-2307Number of pages 6 s. Language eng - English Country JP - Japan Keywords low-neodymium neodymium-iron-boron alloy ; thermomagnetic measurements ; X-ray diffraction ; magnetic properties Subject RIV BM - Solid Matter Physics ; Magnetism R&D Projects 1M0512 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) CEZ AV0Z20410507 - UFM-A (2005-2011) UT WOS 000271242900030 DOI 10.2320/matertrans.M2009138 Annotation Changes in the phase composition and crystallite size of a rapid quenched Nd4.5Fe77B18.5 alloy, caused by thermomagnetic measurements (TM) have been studied using XRD methods of phase analysis. crystallite size and lattice microstrain determination. Structural changes in regard to optimal magnetic state were additionally analyzed by TEM. Magnetic properties in optimal magnetic state and after TM were observed using room temperature SQUID measurements. The obtained experimental results suggest the Fe3B/Nd2Fe14B and partly alpha-Fe nanocomposite structure of the alloy in the optimized magnetic state. with mean crystallite size (< 30nm). After TM. an increased amount of alpha-Fe phase, presence of different oxide and Fe-B phases as well as growth of crystallites are found to be the main reasons for the observed quality loss of hard magnetic properties. Workplace Institute of Physics of Materials Contact Yvonna Šrámková, sramkova@ipm.cz, Tel.: 532 290 485 Year of Publishing 2010
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