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End Effects in Rotational Viscometry I. No-Slip Shear-Thinning Samples in the Z40 DIN Sensor.
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SYSNO ASEP 0091179 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Ostatní články Title End Effects in Rotational Viscometry I. No-Slip Shear-Thinning Samples in the Z40 DIN Sensor. Title Koncové efekty v rotační viskozimetrii I. Měření pseudoplastických vzorků bez skluzu ve viskozimetru Z40 DIN. Author(s) Wein, Ondřej (UCHP-M) RID, SAI
Večeř, Marek (UCHP-M)
Havlica, Jaromír (UCHP-M) RID, ORCID, SAISource Title Rheologica Acta - ISSN 0035-4511
Roč. 46, 5 (2007) , s. 765-772Number of pages 8 s. Action Annual Rheology Conference AERC 2006 /3./ Event date 27.04.2006-29.04.2006 VEvent location Crete Country GR - Greece Event type EUR Language eng - English Country DE - Germany Keywords rotational couette flow ; shear-thinning fluids ; end effects Subject RIV CI - Industrial Chemistry, Chemical Engineering R&D Projects GA104/04/0826 GA ČR - Czech Science Foundation (CSF) GP104/06/P287 GA ČR - Czech Science Foundation (CSF) GP104/05/P554 GA ČR - Czech Science Foundation (CSF) CEZ AV0Z40720504 - UCHP-M (2005-2011) Annotation Neglect of end effects in Couette rotational viscometry introduces 10-30% error in the estimate of shear stress at spindle surface. Actual deviations depend on the shear-thinning level of a given sample. We tackle the end effect for the standard sensor Z40 DIN according to ISO 3219 by solving the related 2D boundary-value problem for a class of shear-thinning viscosity functions. Pseudosimilarity method of treating the primary data leaves an error in shear stresses about 0.5%. Further reduction of the errors needs a full numerical simulation for each point of primary data, based on a suitable wide-range representation of the viscosity function. To support high accuracy of torque calibrations, the effect of inertia on torque for Newtonian liquids in standard sensor Z40 DIN at Re < 500 is calculated using the FLUENT 6.2 commercial software. Workplace Institute of Chemical Process Fundamentals Contact Eva Jirsová, jirsova@icpf.cas.cz, Tel.: 220 390 227 Year of Publishing 2008
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