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Dataset thin film growth of [Ni(Hvanox)2] NanoscaleAdv
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Title of dataset Dataset thin film growth of [Ni(Hvanox)2] NanoscaleAdv Author(s) Sapre, Atharva Umesh (FZU-D) ORCID
Vlček, Jan (FZU-D) RID, ORCID
de Prado, Esther (FZU-D) ORCID, RID
Fekete, Ladislav (FZU-D) RID, ORCID
Klementová, Mariana (FZU-D) RID, ORCID
Vondráček, Martin (FZU-D) RID, ORCID
Svora, Petr (FZU-D) ORCID
Cuza, E. (IE)
Morgan, G.G. (IE)
Honolka, Jan (FZU-D) RID, ORCID
Kühne, Irina A. (FZU-D) ORCIDType of datasets Dataset Language angličtina Description of the dataset We have investigated [Ni(Hvanox)2] (H2vanox = o-vanillinoxime), a square-planar Ni(II) complex, for the preparation of thin films using organic molecule evaporation. Low pressure experiments to prepare thin films were conducted at temperatures between 120–150 °C and thin films of increasing thicknesses [Ni(Hvanox)2] (16–336 nm) have been prepared on various substrates and been analyzed by microscopic and spectroscopic methods. Scanning electron microscopy (SEM), atomic force microscopy (AFM) and transmission electron microscopy (TEM) were used to reveal a rough surface morphology which exhibits a dense arrangement of elongated, rod and needle-like nanocrystals with random orientations. It also enabled us to follow the growth of the thin films by increasing thickness revealing the formation of a seeding layer. X-ray photoelectron spectroscopy (XPS and 3D ED), TEM and X-ray diffraction (XRD) were utilized to confirm the atomic structure and the elemental composition of the thin films.
Funding EH22_008/0004596
GA23-05878S
LM2023051Institutional support RVO:68378271 Keywords thin film * coordination complex * Ni(II) * film growth * thickness dependence License CC BY 4.0 - Attribution-International license Contact person Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 DOI https://doi.org/10.57680/asep.0618314
Handle: https://hdl.handle.net/11104/0365175Record owner Institute of Physics SYSNO 0618314 Date issued 24.03.2025 File Download Size Commentary Access Dataset-thin film growth of [Ni(Hvanox)2]_NanoscaleAdv.zip File list 17 34.9 MB open-access
Number of the records: 1