New dinuclear methoxo-bridged manganese(III) complex: Synthesis, characterization and usage as new precursor for synthesis of Mn.sub.2./sub.O.sub.3./sub. particles

Khalaji, A.D.; Ghorbani, M.; Feizi, N.; Akbari, A.; Dušek, Michal; Eigner, Václav

doi:https://dx.doi.org/10.22059/jsciences.2020.255907.1007246

Number of the records: 1

New dinuclear methoxo-bridged manganese(III) complex: Synthesis, characterization and usage as new precursor for synthesis of Mn.sub.2./sub.O.sub.3./sub. particles

1.

SYSNO ASEP	0537580
Document Type	J - Journal Article
R&D Document Type	Journal Article
Subsidiary J	Článek ve SCOPUS
Title	New dinuclear methoxo-bridged manganese(III) complex: Synthesis, characterization and usage as new precursor for synthesis of Mn₂O₃ particles
Author(s)	Khalaji, A.D. (IR) Ghorbani, M. (IR) Feizi, N. (IR) Akbari, A. (IR) Dušek, Michal (FZU-D)_{RID, ORCID, SAI} Eigner, Václav (FZU-D)_{RID, ORCID}
Number of authors	6
Source Title	Journal of Sciences, Islamic Republic of Iran. - : University of Tehran - ISSN 1016-1104 Roč. 31, č. 1 (2020), s. 33-38
Number of pages	5 s.
Publication form	Print - P
Language	eng - English
Country	IR - Iran
Keywords	dinuclear ; manganese(III) ; Schiff base ; crystal structure ; Mn₂O₃ particles
Subject RIV	BM - Solid Matter Physics ; Magnetism
OECD category	Condensed matter physics (including formerly solid state physics, supercond.)
R&D Projects	GA15-12653S GA ČR - Czech Science Foundation (CSF)
	LO1603 GA MŠMT - Ministry of Education, Youth and Sports (MEYS)
Method of publishing	Open access
Institutional support	FZU-D - RVO:68378271
EID SCOPUS	85093898273
DOI	10.22059/jsciences.2020.255907.1007246
Annotation	New dinuclear methoxo-bridged manganese(III) complex [Mn2((MeObph)en)2Cl2(μ-CH3O)2] (1) was synthesized by template reaction of 2-hydroxy-4-methoxybenzophenone, 1,2-ethanediamine and MnCl2.6H2O with molar ration (1:1:1) in methanol as solvent. The title compound 1 was characterized by elemental analyses (CHN), Fourier Transform infrared spectroscopy (FT-IR) and single crystal X-ray diffraction. Finally, by calcination of 1 at 500 oC for 3 h, we prepared Mn2O3 particles and characterized by FT-IR, XRD and SEM.
Workplace	Institute of Physics
Contact	Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579
Year of Publishing	2021
Electronic address	http://hdl.handle.net/11104/0315404

Number of the records: 1