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Monitoring of enzymatic enantioselective acetylation of gem-difluorinated alcohols by capillary electrophoresis
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SYSNO ASEP 0493508 Document Type C - Proceedings Paper (int. conf.) R&D Document Type The record was not marked in the RIV Title Monitoring of enzymatic enantioselective acetylation of gem-difluorinated alcohols by capillary electrophoresis Author(s) Šolínová, Veronika (UOCHB-X) RID, ORCID
Pomeisl, Karel (UOCHB-X) RID
Lamatová, Nikola (UOCHB-X)
Pohl, Radek (UOCHB-X) RID, ORCID
Brabcová, Jana (UOCHB-X) RID
Krečmerová, Marcela (UOCHB-X) RID, ORCID
Kašička, Václav (UOCHB-X) RID, ORCIDSource Title Advances in Chromatography and Electrophoresis & Chiranal 2018. - Olomouc : Palacký University, 2018 / Bednář P. ; Cechová M. ; Kučera L. ; Kurka O. Pages s. 128-129 Number of pages 2 s. Publication form Print - P Action Advances in Chromatography and Electrophoresis & Chiranal 2018 Event date 29.01.2018 - 01.02.2018 VEvent location Olomouc Country CZ - Czech Republic Event type EUR Language eng - English Country CZ - Czech Republic Keywords enantioselective acetylation ; difluorinated alcohols ; capillary electrophoresis Subject RIV CB - Analytical Chemistry, Separation OECD category Analytical chemistry R&D Projects GA15-01948S GA ČR - Czech Science Foundation (CSF) GA17-10832S GA ČR - Czech Science Foundation (CSF) Institutional support UOCHB-X - RVO:61388963 Annotation A new fast and highly efficient capillary electrophoretic (CE) method has been developed for chiral analysis of non-charged gem-difluorinated alcohol (3-(benzyloxy)-1,1-difluoro-propan-2-ol) using sulfobutylether-β-CD as chiral selector. The method was applied for monitoring of enzymatic (lipase mediated) enantioselective acetylation of the above alcohol and for determination of enantiomeric purity of both substrates and products of the enzymatic reaction. Workplace Institute of Organic Chemistry and Biochemistry Contact asep@uochb.cas.cz ; Kateřina Šperková, Tel.: 232 002 584 ; Jana Procházková, Tel.: 220 183 418 Year of Publishing 2019
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