Characterization and crystal structure of a 17-membered macrocyclic Schiff base compound MeO-sal-pn-bn

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SYSNO ASEP	0456422
Document Type	J - Journal Article
R&D Document Type	Journal Article
Subsidiary J	Článek ve WOS
Title	Characterization and crystal structure of a 17-membered macrocyclic Schiff base compound MeO-sal-pn-bn
Author(s)	Khalaji, A.D. (IR) Ghoran, S.H. (IR) Rohlíček, Jan (FZU-D)_{RID, ORCID} Dušek, Michal (FZU-D)_{RID, ORCID, SAI}
Source Title	Journal of Structural Chemistry. - : Pleiades Publishing - ISSN 0022-4766 Roč. 56, č. 2 (2015), s. 259-265
Number of pages	7 s.
Language	eng - English
Country	RU - Russian Federation
Keywords	macrocyclic ; Schiff base ; spectroscopy ; powder diffraction ; orthorhombic
Subject RIV	BM - Solid Matter Physics ; Magnetism
Institutional support	FZU-D - RVO:68378271
UT WOS	000355235600008
EID SCOPUS	84934873867
DOI	10.1134/S0022476615020080
Annotation	The reaction of 1,4-diaminobutane with 2,2′-diformyl-6,6′-dimethoxy-diphenoxypropane in a mixed solvent of methanol and chloroform results in a new 17-membered macrocyclic Schiff base compound MeO-sal-pn-pn. The title compound is characterized by the elemental analysis (CHN), FT-IR, 1H NMR spectroscopy, and powder X-ray diffraction. The crystal data are: Mr = 396.5, orthorhombic, P212121, with unit cell parameters: a = 4.71769(3) Å, b = 19.1524(2) Å, c = 22.9418(2) Å, V = 2072.90(3) Å3, and Z = 4.
Workplace	Institute of Physics
Contact	Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579
Year of Publishing	2016

Number of the records: 1