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Suspension polymerization of aniline hydrochloride in non-aqueous media
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SYSNO ASEP 0359118 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Suspension polymerization of aniline hydrochloride in non-aqueous media Author(s) Konyushenko, Elena (UMCH-V) RID, ORCID
Stejskal, Jaroslav (UMCH-V) RID, ORCID, SAI
Trchová, Miroslava (UMCH-V) RID, ORCID
Prokeš, J. (CZ)Source Title Polymer International. - : Wiley - ISSN 0959-8103
Roč. 60, č. 5 (2011), s. 794-797Number of pages 4 s. Language eng - English Country GB - United Kingdom Keywords conducting polymer ; polyaniline ; non-aqueous media Subject RIV CD - Macromolecular Chemistry R&D Projects IAA400500905 GA AV ČR - Academy of Sciences of the Czech Republic (AV ČR) IAA100500902 GA AV ČR - Academy of Sciences of the Czech Republic (AV ČR) CEZ AV0Z40500505 - UMCH-V (2005-2011) UT WOS 000289516300012 DOI 10.1002/pi.3017 Annotation The oxidation of aniline hydrochloride by ammonium peroxydisulfate in non-aqueous media was studied, when themonomer or oxidant or both were not completely soluble. Polyaniline was formed in acetone, methanol and toluene. Aniline oligomers only were produced in chloroform and n-butylacetate. No interaction of the monomer and the oxidant was observed in dimethylsulfoxide and N-methylpyrrolidone. UV-visible and Fourier transform infrared spectra were recorded in order to study themolecular structure of the final products. Conductivity was measured for conducting protonated forms and corresponding bases. An explanation of aniline hydrochloride oxidation in various organicmedia is offered. Workplace Institute of Macromolecular Chemistry Contact Eva Čechová, cechova@imc.cas.cz ; Tel.: 296 809 358 Year of Publishing 2012
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