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A new route to the syntheses of N-(fluorosulfuryl)sulfonamide salts: Crystal structure of Ph4P+ [CF3SO2NSO2F]
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SYSNO ASEP 0341016 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title A new route to the syntheses of N-(fluorosulfuryl)sulfonamide salts: Crystal structure of Ph4P+ [CF3SO2NSO2F] Author(s) Beran, Martin (UIACH-O)
Příhoda, J. (CZ)
Taraba, J. (CZ)Number of authors 3 Source Title Polyhedron. - : Elsevier - ISSN 0277-5387
Roč. 29, č. 3 (2010), s. 991-994Number of pages 4 s. Language eng - English Country NL - Netherlands Keywords N-(fluorosulfuryl) sulfonamides ; N-(fluorosulfuryl)trifluoromethane sulfonamide ; N-(chlorosulfuryl)trifluoromethane Subject RIV CB - Analytical Chemistry, Separation CEZ AV0Z40310501 - UIACH-O (2005-2011) UT WOS 000275640700006 DOI 10.1016/j.poly.2009.11.024 Annotation A new route for the preparation of potassium and tetraphenylphosphonium salts of N-(fluorosulfuryl)trifluoromethane sulfonamide is described. N-(chlorosulfuryl)-trifluoromethane sulfonamide CF3SO2–NH– SO2Cl, that was used for preparations of both salts, was prepared by the reaction of trifluoromethane sulfonamide CF3SO2NH2 and chlorosulfonic acid in the presence of SOCl2. Workplace Institute of Analytical Chemistry Contact Iveta Drobníková, drobnikova@iach.cz, Tel.: 532 290 234 Year of Publishing 2010
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