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Preparation and characterization of alumina submicron fibers by plasma assisted calcination
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SYSNO ASEP 0536709 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Preparation and characterization of alumina submicron fibers by plasma assisted calcination Author(s) Medvecká, V. (SK)
Kováčik, D. (SK)
Stupavská, M. (CZ)
Roch, T. (SK)
Kromka, Alexander (FZU-D) RID, ORCID, SAI
Fajgar, Radek (UCHP-M) RID, ORCID, SAI
Zahoranová, A. (SK)
Černák, M. (CZ)Number of authors 8 Source Title Ceramics International. - : Elsevier - ISSN 0272-8842
Roč. 46, č. 14 (2020), s. 22774-22780Number of pages 7 s. Language eng - English Country GB - United Kingdom Keywords Al2O3 submicron fibres ; plasma-assisted calcination ; coplanar discharge ; dielectric barrier discharge ; atmospheric pressure plasma Subject RIV BL - Plasma and Gas Discharge Physics OECD category Materials engineering Subject RIV - cooperation Institute of Chemical Process Fundamentals - Plasma and Gas Discharge Physics R&D Projects LM2018110 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) Method of publishing Open access with time embargo (01.10.2022) Institutional support FZU-D - RVO:68378271 ; UCHP-M - RVO:67985858 UT WOS 000558707400100 EID SCOPUS 85086517808 DOI 10.1016/j.ceramint.2020.06.044 Annotation Ceramic alumina nanofibers were prepared by plasma-assisted calcination (PAC) using atmospheric pressure plasma. Electrospun polyvinyl pyrrolidone/aluminium butoxide fibers were pre-treated by plasma generated in ambient air using a special type of coplanar dielectric barrier discharge. The effect of plasma on fibers and structural, chemical and crystalline properties of obtained ceramic nanofibers were characterized using XPS and SEM, EDX and XRD. Thermogravimetric and differential thermal analysis were used for the study of thermal behaviour of untreated and plasma-treated samples. The ceramic fibers prepared by PAC exhibit suitable chemical composition, higher porosity, high length of fibers and better crystalline properties with simultaneous simplifying of the sintering process. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2021 Electronic address https://doi.org/10.1016/j.ceramint.2020.06.044
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