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Kinetic study of static recrystallization in an Fe–Al–O ultra-fine-grained nanocomposite
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SYSNO ASEP 0482161 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Kinetic study of static recrystallization in an Fe–Al–O ultra-fine-grained nanocomposite Author(s) Bártková, Denisa (UFM-A)
Šmíd, Miroslav (UFM-A) RID, ORCID
Mašek, B. (CZ)
Svoboda, Jiří (UFM-A) RID, ORCID
Šiška, Filip (UFM-A) RID, ORCIDNumber of authors 5 Source Title Philosophical Magazine Letters. - : Taylor & Francis - ISSN 0950-0839
Roč. 97, č. 10 (2017), s. 379-385Number of pages 7 s. Language eng - English Country GB - United Kingdom Keywords recrystallization ; dislocation structures ; nanoscale precipitates ; microstructure ; abrupt grain coarsening Subject RIV JL - Materials Fatigue, Friction Mechanics OECD category Audio engineering, reliability analysis R&D Projects GJ15-21292Y GA ČR - Czech Science Foundation (CSF) LM2015069 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) Institutional support UFM-A - RVO:68081723 UT WOS 000419398100001 EID SCOPUS 85029901914 DOI 10.1080/09500839.2017.1378445 Annotation A nearly abrupt coarsening of grains is observed in a newly developed Fe–Al–O ultra-fine-grained nanocomposite with a significant volume fraction (4%) of alumina nano-precipitates. The microstructure of the alloy was analysed in different states (as-received and annealed) by means of scanning electron microscopy, transmission electron microscopy (TEM) and hardness. The initial grain size 150–200 nm increases up to 50 micrometers during annealing 1000 °C/8 h and thereafter demonstrates saturation. A linear correlation between volume fraction of coarse grains and hardness was found. It was identified by TEM that alumina nano-precipitates stabilize the dislocation microstructure against recovery very effectively and the grain coarsening is due to fast growth of very few dislocation free grains. Thus, the observed grain coarsening has the attributes of static recrystallization. Workplace Institute of Physics of Materials Contact Yvonna Šrámková, sramkova@ipm.cz, Tel.: 532 290 485 Year of Publishing 2018
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