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Synthesis of dense yttrium-stabilised hafnia pellets for nuclear applications by spark plasma sintering

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    SYSNO ASEP0439262
    Document TypeJ - Journal Article
    R&D Document TypeJournal Article
    Subsidiary JČlánek ve WOS
    TitleSynthesis of dense yttrium-stabilised hafnia pellets for nuclear applications by spark plasma sintering
    Author(s) Tyrpekl, V. (DE)
    Holzhdauser, M. (DE)
    Hein, H. (DE)
    Vigier, J.F. (DE)
    Somers, J. (DE)
    Svora, Petr (UACH-T) SAI
    Source TitleJournal of Nuclear Materials. - : Elsevier - ISSN 0022-3115
    Roč. 454, 1-3 (2014), s. 398-404
    Number of pages7 s.
    Languageeng - English
    CountryNL - Netherlands
    KeywordsNuclear application ; Sol-gel ; Zirconia ; Transmutation ; Fabrication ; Actinides
    Subject RIVCA - Inorganic Chemistry
    Institutional supportUACH-T - RVO:61388980
    UT WOS000344428900052
    EID SCOPUS84908222068
    DOI10.1016/j.jnucmat.2014.08.029
    AnnotationDense yttrium-stabilised hafnia pellets (91.35 wt.% HfO2 and 8.65 wt.% Y2O3) were prepared by spark plasma sintering consolidation of micro-beads synthesised by the "external gelation" sol-gel technique. This technique allows a preparation of HfO2-Y2O3 beads with homogenous yttria-hafnia solid solution. A sintering time of 5 min at 1600 degrees C was sufficient to produce high density pellets (over 90% of the theoretical density) with significant reproducibility. The pellets have been machined in a lathe to the correct dimensions for use as neutron absorbers in an experimental test irradiation in the High Flux Reactor (HFR) in Petten, Holland, in order to investigate the safety of americium based nuclear fuels.
    WorkplaceInstitute of Inorganic Chemistry
    ContactJana Kroneislová, krone@iic.cas.cz, Tel.: 311 236 931
    Year of Publishing2015
Number of the records: 1  

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