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Copper(II), nickel(II), zinc(II) and vanadium(IV) Schiff base complexes: synthesis, characterization, crystal structure determination, and thermal studies
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SYSNO ASEP 0498352 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Copper(II), nickel(II), zinc(II) and vanadium(IV) Schiff base complexes: synthesis, characterization, crystal structure determination, and thermal studies Author(s) Barfeie, H. (IR)
Grivani, G. (IR)
Eigner, Václav (FZU-D) RID, ORCID
Dušek, Michal (FZU-D) RID, ORCID, SAI
Khalaji, A.D. (IR)Number of authors 5 Source Title Polyhedron. - : Elsevier - ISSN 0277-5387
Roč. 146, May (2018), s. 19-25Number of pages 7 s. Publication form Print - P Language eng - English Country GB - United Kingdom Keywords Schiff base ; complex ; thermal study ; nanoparticle ; naphthaldimine Subject RIV BM - Solid Matter Physics ; Magnetism OECD category Condensed matter physics (including formerly solid state physics, supercond.) R&D Projects GA15-12653S GA ČR - Czech Science Foundation (CSF) LO1603 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) Institutional support FZU-D - RVO:68378271 UT WOS 000431157400003 EID SCOPUS 85042933244 DOI 10.1016/j.poly.2018.02.012 Annotation Four new bis-chelate ML2 complexes (M = Cu2+, Ni2+, Zn2+, VO2+ and L = 1-[Furan-2-(ylmethylimino)methyl]naphthalene-2-olate) with bidentate NO Schiff base ligand were synthesized and characterized by spectral and analytical techniques. The crystal structures of CuL2, NiL2, and VOL2 were determined by single crystal X-ray analysis. In all cases, two Schiff base ligands bind to the metal centers in the trans O–M–N manner. Thermal analysis and thermal decomposition of the titled complexes were investigated. The data of TGA, XRD and SEM analyses revealed that they were converted to corresponding metal oxides in a form of nanoparticles. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2019
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