AFM and SEM-FEG study on fundamental mechanisms leading to fatigue crack initiation

0453925 - ÚFM 2016 RIV GB eng J - Journal Article
Man, Jiří - Valtr, M. - Petrenec, Martin - Dluhoš, J. - Kuběna, Ivo - Obrtlík, Karel - Polák, Jaroslav
AFM and SEM-FEG study on fundamental mechanisms leading to fatigue crack initiation.
International Journal of Fatigue. Roč. 76, JUL (2015), s. 11-18. ISSN 0142-1123. E-ISSN 1879-3452
R&D Projects: GA ČR(CZ) GAP108/10/2371; GA MŠMT(CZ) ED1.1.00/02.0068; GA ČR(CZ) GA13-23652S
Institutional support: RVO:68081723
Keywords : fatigue crack initiation * 316L austenitic steel * atomic force microscopy * extrusion * intrusion
Subject RIV: JL - Materials Fatigue, Friction Mechanics
Impact factor: 2.162, year: 2015

Early stages of surface relief evolution of persistent slip markings (PSMs) in polycrystalline 316L austenitic stainless steel cycled with constant plastic strain amplitude at 93, 173 and 573 K were studied using atomic force microscopy (AFM) and high-resolution scanning electron microscopy (SEM-FEG). Qualitative and quantitative data on the morphology of PSMs, occurrence of extrusions and intrusions and the kinetics of extrusion growth are reported for all temperatures. PSMs start in all cases as surface extrusions which are later accompanied by formation of intrusions. This finding is discussed with respect to the point defect formation within areas of localized cyclic slip and primarily to their mobility at different temperatures. Consequences of migration of respective point defects for surface relief formation and the conditions for creation of fatigue crack embryos, i.e. sharp intrusions are highlighted.
Permanent Link: http://hdl.handle.net/11104/0254671