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Epoxy catalyzed sol–gel method for pinhole-free pyrite FeS.sub.2./sub. thin films

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    0440633 - FZÚ 2015 RIV NL eng J - Journal Article
    Kment, Štěpán - Kmentová, Hana - Sarkar, A. - Soukup, R. J. - Ianno, N.J. - Sekora, D. - Olejníček, Jiří - Kšírová, Petra - Krysa, J. - Remeš, Zdeněk - Hubička, Zdeněk
    Epoxy catalyzed sol–gel method for pinhole-free pyrite FeS2 thin films.
    Journal of Alloys and Compounds. Roč. 607, Sep (2014), s. 169-176. ISSN 0925-8388. E-ISSN 1873-4669
    R&D Projects: GA MŠMT LH12043
    Grant - others:AV ČR(CZ) M100101215
    Institutional support: RVO:68378271 ; RVO:67985858
    Keywords : heterojunction * photoelectrochemical solar cells * sol-gel * thin films
    Subject RIV: JJ - Other Materials
    Impact factor: 2.999, year: 2014

    The uniform pinhole-free iron disulfide (FeS2) pyrite thin films were fabricated. In the first step the FeO(OH)x xerogel solution was synthetized by means of a novel epoxy catalyzed sol–gel method and next spin-coated onto various substrates to form the thin films. In the second step the xerogel coatings were annealed to yield hematite(Alpha-Fe2O3) films, which were transformed into pyrite by chemical sulfurization. Among the main deposition parameters studied were the temperature of xerogel–hematite transformation and the optimalsufulrization temperature and duration.
    Permanent Link: http://hdl.handle.net/11104/0243757

     
     
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