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Rerefinement of poly[di­aqua­bis­­(μ.sub.3./sub.-2-methyl­pro­pano­ato-κ.sup.4./sup.O:O,O′:O′)bis­­(μ.sub.3./sub.-2-methyl­propano­ato-κ.sup.3./sup.O:O:O)(μ.sub.2./sub.-2-methyl­propano­ato-κ.sup.3./sup.O:O,O′)(2-methyl­propano­ato-κ.sup.2./sup.O,O′)trilead(II)].

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    0537643 - FZÚ 2021 RIV GB eng J - Journal Article
    Samoľová, Erika - Fábry, Jan
    Rerefinement of poly[di­aqua­bis­­(μ3-2-methyl­pro­pano­ato-κ4O:O,O′:O′)bis­­(μ3-2-methyl­propano­ato-κ3O:O:O)(μ2-2-methyl­propano­ato-κ3O:O,O′)(2-methyl­propano­ato-κ2O,O′)trilead(II)].
    IUCrData. Roč. 5, č. 10 (2020), s. 1-3, č. článku x201311. E-ISSN 2414-3146
    R&D Projects: GA MŠMT(CZ) LO1603
    Institutional support: RVO:68378271
    Keywords : crystal structure * hydrogen bonding * carboxylates * The Cambridge Structural Database
    OECD category: Condensed matter physics (including formerly solid state physics, supercond.)
    Method of publishing: Open access

    The crystal structure of the title complex, [Pb3(C4H7O2)6(H2O)2]n, was redetermined on basis of modern CCD-based single-crystal X-ray data at 120 K. The current study basically confirms the previous report at 190 K, but with higher accuracy and precision. In particular, positional disorder of one of the 2-methylpropanoate anions over two sets of sites was resolved.

    Permanent Link: http://hdl.handle.net/11104/0315453

     
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