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Structure and properties of nano- and polycrystalline Mn-doped CuCr.sub.2./sub.Se.sub.4./sub. obtained by ceramic method and high-energy ball milling
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SYSNO ASEP 0541669 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Structure and properties of nano- and polycrystalline Mn-doped CuCr2Se4 obtained by ceramic method and high-energy ball milling Author(s) Jendrzejewska, I. (PL)
Knížek, Karel (FZU-D) RID, ORCID
Kubacki, J. (PL)
Goraus, J. (PL)
Goryczka, T. (PL)
Pietrasik, E. (PL)
Barsova, Z. (PL)
Jampílek, J. (SK)
Witkowska-Kita, B. (PL)Number of authors 9 Article number 111174 Source Title Materials Research Bulletin. - : Elsevier - ISSN 0025-5408
Roč. 137, May (2021)Number of pages 13 s. Language eng - English Country GB - United Kingdom Keywords inorganic compounds ; magnetic properties ; XRD ; DSC/TG and XPS ; photoelectron spectroscopy ; electronic structure Subject RIV BM - Solid Matter Physics ; Magnetism OECD category Condensed matter physics (including formerly solid state physics, supercond.) R&D Projects LM2018096 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) Method of publishing Limited access Institutional support FZU-D - RVO:68378271 UT WOS 000619678700006 EID SCOPUS 85098592475 DOI 10.1016/j.materresbull.2020.111174 Annotation Chemical compounds with a general formula CuCr2-xMnxSe4 (x = 0.1, 0.2)were successfully synthesized in polycrystalline form, using solid state reaction method, and as nanoparticles, using high-energy ball milling.The influence of manganese and grain size on their structure, magnetic and thermal properties was investigated by X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM),magnetic measurements (SQUID, high magnetic fields) and DSC (Differential Scanning Calorimetry). Electronic structures of obtained compounds were determined using XANES (X-ray Near Edge Absorption Spectroscopy) and XPS (X-ray Photoelectron Spectroscopy).X-ray studies confirmed that the spinel phase forms only for x = 0.1, 0.2. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2022 Electronic address https://doi.org/10.1016/j.materresbull.2020.111174
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