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Synthesis, characterization and thermal studies of a nanosized 1D L-Arginine/Copper(II) coordination polymer by sonochemical method: a new precursor for preparation of copper(II) oxide nanoparticles
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SYSNO ASEP 0533714 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Synthesis, characterization and thermal studies of a nanosized 1D L-Arginine/Copper(II) coordination polymer by sonochemical method: a new precursor for preparation of copper(II) oxide nanoparticles Author(s) Alikhani, M. (IR)
Hakimi, M. (IR)
Moeini, K. (IR)
Eigner, Václav (FZU-D) RID, ORCID
Dušek, Michal (FZU-D) RID, ORCID, SAINumber of authors 5 Source Title Journal of Inorganic and Organometallic Polymers and Materials. - : Springer - ISSN 1574-1443
Roč. 30, č. 8 (2020), s. 2907-2915Number of pages 8 s. Language eng - English Country US - United States Keywords coordination polymer ; copper(II) ; L-Arginine ; crystal structure ; thermal decomposition ; nanoparticles Subject RIV BM - Solid Matter Physics ; Magnetism OECD category Condensed matter physics (including formerly solid state physics, supercond.) R&D Projects LO1603 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) GA18-10504S GA ČR - Czech Science Foundation (CSF) Method of publishing Limited access Institutional support FZU-D - RVO:68378271 UT WOS 000547945500009 EID SCOPUS 85077624373 DOI 10.1007/s10904-020-01442-8 Annotation In the present work, 1D-copper(II) coordination polymer, {[Cu(μ-l-Arg)2(H2O)]SO4}n (1), (l-Arg: l-Arginine), was synthesized and identified by elemental analysis, FT-IR spectroscopy, molar conductivity, thermal gravimetric analysis (TGA), differential thermal analysis (DTA) and single-crystal X-ray diffraction. The compound 1 was also prepared by a sonochemical process in the form of nanoparticles. The particle size and morphology of the synthesized nanoparticles were investigated by powder X-ray diffraction (PXRD) and field emission scanning electron microscopy (FE-SEM). Finally, CuO nanoparti cles were produced by thermal decomposition of the sonochemically prepared nanoparticles of 1, and characterized by FT-IR, XRD, FE-SEM and EDS. Workplace Institute of Physics Contact Kristina Potocká, potocka@fzu.cz, Tel.: 220 318 579 Year of Publishing 2021 Electronic address https://doi.org/10.1007/s10904-020-01442-8
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