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Synthesis of nanostructured TiO2 (anatase) and TiO2(B) in ionic liquids
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SYSNO ASEP 0427477 Document Type J - Journal Article R&D Document Type Journal Article Subsidiary J Článek ve WOS Title Synthesis of nanostructured TiO2 (anatase) and TiO2(B) in ionic liquids Author(s) Mansfeldová, Věra (UFCH-W) RID
Lásková, Barbora (UFCH-W) RID
Krýsová, Hana (UFCH-W) RID, ORCID
Zukalová, Markéta (UFCH-W) RID, SAI, ORCID
Kavan, Ladislav (UFCH-W) RID, ORCIDSource Title Catalysis Today. - : Elsevier - ISSN 0920-5861
Roč. 230, JUL 2014 (2014), s. 85-90Number of pages 6 s. Language eng - English Country NL - Netherlands Keywords TiO2(B) ; ionic liquid ; electrochemistry Subject RIV CG - Electrochemistry R&D Projects GA13-07724S GA ČR - Czech Science Foundation (CSF) 7E09117 GA MŠMT - Ministry of Education, Youth and Sports (MEYS) Institutional support UFCH-W - RVO:61388955 UT WOS 000333800300015 EID SCOPUS 84897581316 DOI 10.1016/j.cattod.2014.01.007 Annotation Sol-gel synthesis of TiO2 (anatase) and TiO2(B) was carried out in the presence of imidazolium based ionic liquids with tetrafluoroborate and chloride ions. The prepared nanoparticles were characterized by cyclic voltammetry, Raman spectroscopy and scanning electron microscopy. The influence of organic solvent type and synthesis atmosphere on the product's composition was evaluated. It was established that a nitrogen atmosphere favours the growth of anatase crystalline phase and inhibits the formation of TiO2(B). Workplace J. Heyrovsky Institute of Physical Chemistry Contact Michaela Knapová, michaela.knapova@jh-inst.cas.cz, Tel.: 266 053 196 Year of Publishing 2015
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