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Synthesis of Mono(perfluoroalkyl) Cyclodextrins via Cross Metathesis

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    0355716 - ÚOCHB 2011 RIV DE eng J - Journal Article
    Řezanka, M. - Eignerová, Barbara - Jindřich, J. - Kotora, M.
    Synthesis of Mono(perfluoroalkyl) Cyclodextrins via Cross Metathesis.
    European Journal of Organic Chemistry. -, č. 32 (2010), s. 6256-6262. ISSN 1434-193X. E-ISSN 1099-0690
    R&D Projects: GA AV ČR KAN200200651
    Institutional research plan: CEZ:AV0Z40550506
    Keywords : metathesis * cyclodextrins * fluorine * alkylation * amphiphiles
    Subject RIV: CC - Organic Chemistry
    Impact factor: 3.206, year: 2010

    Ruthenium–carbene complex catalyzed cross metathesis of monoallyl alpha-, beta-, and gamma-cyclodextrins with perfluoroalkylpropenes resulted in the formation of the corresponding perfluoroalkylated cyclodextrins. The reactions proceeded under standard reaction conditions and yielded the desired compounds in reasonable yields. Dynamic light scattering measurements proved the ability of the prepared compounds to aggregate in water solution forming nanoparticles in the range of tens and thousands of nanometers.
    Permanent Link: http://hdl.handle.net/11104/0194418

     
     
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