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Neutron activation analysis with pre- and post-irradiation chemical separation for the value assignments of Al, V, and Ni in the new bovine liver SRM 1577C

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    0339307 - ÚJF 2010 RIV HU eng J - Journal Article
    Zeisler, R. - Tomlin, B. E. - Murphy, K. E. - Kučera, Jan
    Neutron activation analysis with pre- and post-irradiation chemical separation for the value assignments of Al, V, and Ni in the new bovine liver SRM 1577C.
    Journal of Radioanalytical and Nuclear Chemistry. Roč. 282, č. 1 (2009), s. 69-74. ISSN 0236-5731. E-ISSN 1588-2780
    Institutional research plan: CEZ:AV0Z10480505
    Keywords : Blank contributions * Bovine liver * Low-level trace elements
    Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders
    Impact factor: 0.631, year: 2009

    Instrumental neutron activation analysis as carried out at the National Institute of Standards and Technology (NIST) is inadequate for determining Al, Ni, and V at the levels found in the newly prepared Standard Reference Material(A (R)) (SRM) 1577c Bovine Liver. To overcome shortcomings in the value assignment, the authors initiated a cooperative approach using NAA with previously established chemical separation procedures and with significantly different neutron energy spectra to determine Al and V with pre-irradiation separation of the elements at NIST, and V and Ni with post-irradiation separation at the Nuclear Physics Institute A similar to eA3/4. The determinations were confirmed with the analyses of several SRMs. The work supported the certification of mass fraction values for V and Ni in SRM 1577c.
    Permanent Link: http://hdl.handle.net/11104/0005732

     
     
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